Fertiliser Analysis

 

Interlaboratory Tests by Section III – Fertiliser Analysis

Section III – Fertiliser Analysis – regularly conducts interlaboratory tests for the purpose of quality assurance and for validating and reviewing analytical methods.
Over the past 25 years, this group has carried out internal interlaboratory tests to validate and assure the quality of assay methods for macronutrients and micronutrients, pollutants, nitrification inhibitors and other compounds. Tests performed in recent years include:

  • Interlaboratory test to validate the assay methods for “organic compounds” and “organic carbon” in organic and organic-mineral fertilisers,
  • Chromium VI in ashes,
  • Selenium, arsenic and mercury in mineral fertilisers,
  • ICP-OES for macro-elements and trace elements in different types of fertilisers,
  • Fluorine in sewage sludge and lime (Ziegeleikalk)
  • Carbonates in lime and fertilisers containing lime,
  • Total nitrogen and available nitrogen and
  • Total phosphorus and potassium concentration in agricultural fertilisers

Since 2009, section III has offered an “VDLUFA EU Fertiliser Ring-Test” every year for EU accredited fertiliser testing laboratories in all countries. By participating in these test, laboratories can verify and document the quality of their analysis procedures. Between 28 and 48 laboratories from 21 member states and Turkey have participated over the past five years. To date, 9 interlaboratory tests have been performed on the following fertilisers:

  • 2009: NPK fertiliser containing sulphur,
  • 2010: Carbonic magnesium lime,
  • 2011: NPK fertiliser containing isobutylene urea and micronutrients,
  • 2012: Kornkali fertiliser,
  • 2013: NPK fertiliser,
  • 2014: NP fertiliser,
  • 2015: Liquid micronutrient fertiliser,
  • 2016: Magnesium calcium carbonate (dolomitic limestone),
  • 2017: Calcium ammonium nitrate (CAN 27) and Urea 46.
  • 2018 Organic NPK fertilizer
  • 2018 Mineral fertilizer with potassium chloride
  • 2019 Mineral fertilizer with triple superphosphate
  • 2019 Organic NPK fertilizer (organic compost)
  • 2020 Mineral fertilizer with trace elements
  • 2020 Organic NPK fertilizer
  • 2021 Wood ash fertilizer (mineral K fertilizer with micronutrients)
  • 2022 PK fertilizer with rock phosphate
  • 2023 Liquid mineral NPK fertilizer with trace elements

The range of tests includes main and trace nutrients (different forms of nitrogen, different forms of solubility for other nutrients and inorganic pollutants) according to test methods of the EU Fertilizer Regulation (VO(EC) 2003/2003), VDLUFA methods as well as EN and ISO standards. Participants receive a certificate documenting their performance in the various analyses. In Germany, the accreditation bodies require certificates from the testing laboratories about their successful participation in qualified fertilizer ring tests.